iCloud storage
I have upgraded my iCloud storage but my photos won’t upload though there is 150 free GB.
iPhone 11 Pro
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Try Settings/Your Name/iCloud and slide off Photos syncing. Wait a few minutes and then slide syncing on. Allow time for syncing to occur. The photos sync is extremely slow. It could take several days or more for the photos to sync.
Last resort - have you tried signing out of iCloud, restarting the device, and then signing back in?